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2EB6

Crystal structure of HpcG complexed with Mg ion

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2006-11-12
DetectorADSC QUANTUM 315
Wavelength(s)1.00
Spacegroup nameP 43 21 2
Unit cell lengths135.955, 135.955, 194.064
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 1.690
R-factor0.19532
Rwork0.194
R-free0.21270
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2EB4(apo-HpcG)
RMSD bond length0.007
RMSD bond angle1.037
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.750
High resolution limit [Å]1.6901.700
Rmerge0.0860.261
Number of reflections195362
<I/σ(I)>22
Completeness [%]97.196.2
Redundancy5.84.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP62937% PEG 12000, 0.1M MES, 0.7M potassium thiocyanate, 7% PEG 550 MME, 10mM DTT, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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