2E2P
Crystal structure of Sulfolobus tokodaii hexokinase in complex with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Detector technology | CCD |
Collection date | 2004-12-06 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 82.683, 50.043, 83.192 |
Unit cell angles | 90.00, 114.80, 90.00 |
Refinement procedure
Resolution | 41.720 - 2.000 |
R-factor | 0.183 |
Rwork | 0.183 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2e2o |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 42187 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |