Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1995-10 |
| Detector | RIGAKU RAXIS |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 63.900, 63.900, 109.300 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 7.000 - 1.900 |
| R-factor | 0.0171 * |
| Rwork | 0.171 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 22.500 * |
| Data reduction software | R-AXIS |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 * | |
| High resolution limit [Å] | 1.900 * | 2.000 * |
| Rmerge | 0.045 | |
| Total number of observations | 41868 * | |
| Number of reflections | 14788 | |
| Completeness [%] | 78.0 | 52 * |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 3 (mg/ml) | |
| 2 | 1 | drop | 0.5 (mM) | ||
| 3 | 1 | drop | Tris-HCl | 50 (mM) | |
| 4 | 1 | drop | ammonium sulfate | 1.0 (M) | |
| 5 | 1 | drop | 2-mercaptoethanol | 20 (mM) | |
| 6 | 1 | reservoir | ammonium sulfate | 2.0 (M) | |
| 7 | 1 | reservoir | Tris-HCl | 0.1 (M) |
