2DPH

Crystal Structure of Formaldehyde dismutase

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL38B1
Synchrotron site	SPring-8
Beamline	BL38B1
Temperature [K]	100
Detector technology	CCD
Collection date	2002-02-06
Detector	ADSC QUANTUM 4
Wavelength(s)	1.2736, 1.2832, 1.2827
Spacegroup name	I 41
Unit cell lengths	90.229, 90.229, 226.689
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.920 - 2.270
R-factor	0.209
Rwork	0.207
R-free	0.25000
Structure solution method	MAD
RMSD bond length	0.009
RMSD bond angle	1.273
Data scaling software	d*TREK
Phasing software	MLPHARE
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	41.920	2.350
High resolution limit [Å]	2.270	2.270
Rmerge	0.059	0.201
Number of reflections	41519
<I/σ(I)>	8.7	3
Completeness [%]	99.8	99.3
Redundancy	3.77	3.33

Crystallization Conditions

crystal ID	method	pH	temperature	details
1