2DLI
KILLER IMMUNOGLOBULIN RECEPTOR 2DL2,TRIGONAL FORM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X9B |
Synchrotron site | NSLS |
Beamline | X9B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 91.300, 91.300, 61.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.900 |
R-factor | 0.227 * |
Rwork | 0.227 |
R-free | 0.33100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1nkr |
RMSD bond length | 0.006 |
RMSD bond angle | 26.300 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.063 * | 0.236 * |
Number of reflections | 6169 | |
<I/σ(I)> | 13 | |
Completeness [%] | 90.3 * | 75.4 * |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.5 | pH 6.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | calcium acetate | 250 (mM) | |
2 | 1 | reservoir | PEG8000 | 6 (%) | |
3 | 1 | reservoir | sodium cacodylate | 33 (mM) |