2DHC

CRYSTALLOGRAPHIC ANALYSIS OF THE CATALYTIC MECHANISM OF HALOALKANE DEHALOGENASE

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	94.900, 72.800, 41.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 2.390 *
R-factor	0.195
RMSD bond length	0.014
RMSD bond angle	3.900
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.390 *
Rmerge	0.124 *
Total number of observations	34590 *
Number of reflections	11326 *
Completeness [%]	94.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		60 (%(w/v)sat)
2	1	reservoir	bis-Tris	100 (mM)