2D95
LOW-TEMPERATURE STUDY OF THE A-DNA FRAGMENT D(GGGCGCCC)
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 115 |
| Detector technology | DIFFRACTOMETER |
| Detector | RIGAKU AFC-5 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 42.740, 42.740, 24.570 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 2.000 |
| R-factor | 0.21 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| Number of reflections | 1694 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7 | 115 * | pH 7.00, VAPOR DIFFUSION, temperature 292.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | MGCL2 | ||
| 5 | 1 | 2 | WATER | ||
| 6 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | MPD | 30 (%(v/v)) | ||
| 2 | 1 | cacodylate | 50 (mM) |
