2D5I

The crystal structure of AzoR (Azo Reductase) from Escherichia coli

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-6A
Synchrotron site	Photon Factory
Beamline	BL-6A
Detector technology	CCD
Detector	ADSC QUANTUM 4
Spacegroup name	P 4 21 2
Unit cell lengths	94.630, 94.630, 54.120
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	67.420 - 2.200
R-factor	0.17
Rwork	0.168
R-free	0.20507
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.031
RMSD bond angle	2.175
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	67.420
High resolution limit [Å]	2.200
Number of reflections	12145

Crystallization Conditions

crystal ID	method	pH	temperature	details
1