2D52
Pentaketide chromone synthase (M207G mutant complexed with Coa)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Detector technology | CCD |
Collection date | 2005-02-24 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.070, 89.170, 70.770 |
Unit cell angles | 90.00, 95.72, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
Rwork | 0.193 |
R-free | 0.20800 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 114348 |
Completeness [%] | 94.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |