Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL26B1 |
| Synchrotron site | SPring-8 |
| Beamline | BL26B1 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-11-27 |
| Detector | RIGAKU RAXIS V |
| Wavelength(s) | 0.8, 0.97884, 0.97934, 0.984 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.878, 106.367, 168.639 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.800 |
| R-factor | 0.1816 |
| Rwork | 0.182 |
| R-free | 0.20000 |
| Structure solution method | MAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.270 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 139102 | |
| Completeness [%] | 97.0 | 91.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.1 | 295 | PEG 4K, 0.1M Tris HCl, 1M Lithium Chlorate, MICROBATCH, temperature 295.0K, pH 8.10 |
