2CLR

THREE DIMENSIONAL STRUCTURE OF A PEPTIDE EXTENDING OUT ONE END OF A CLASS I MHC BINDING SITE

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	50.410, 62.909, 74.810
Unit cell angles	81.99, 76.43, 78.06

Refinement procedure

Resolution	6.000 - 2.000
R-factor	0.236
Rwork	0.236
R-free	0.29900 *
RMSD bond length	0.009
RMSD bond angle	2.340
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.900 *	2.070 *
Rmerge	0.054 *	0.205 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	drop	2-(N-morpholino)ethanesulfonic acid	25 (mM)	or 100mM imidazole
3	1	reservoir	PEG6000	15 (%(w/v))