2CFS

crystal structure of human pyridoxal 5'-phosphate phosphatase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 6B
Synchrotron site	PAL/PLS
Beamline	6B
Temperature [K]	100
Detector technology	CCD
Collection date	2005-02-02
Detector	ADSC CCD
Spacegroup name	P 43 21 2
Unit cell lengths	54.631, 54.631, 213.985
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.640 - 2.400
R-factor	0.212
Rwork	0.207
R-free	0.25700
Structure solution method	OTHER
RMSD bond length	0.013
RMSD bond angle	1.444
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.400
Rmerge	0.060
Number of reflections	13489
<I/σ(I)>	33
Completeness [%]	100.0
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1