2CF6

Crystal Structures of the Arabidopsis Cinnamyl Alcohol Dehydrogenases AtCAD5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	277
Spacegroup name	P 41 21 2
Unit cell lengths	54.710, 54.710, 303.930
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.600
R-factor	0.201
Rwork	0.201
R-free	0.23000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1uuf
RMSD bond length	0.012
RMSD bond angle	3.463
Phasing software	AMoRE
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.600
Rmerge	0.060
Number of reflections	14177
<I/σ(I)>	4.4
Completeness [%]	93.2
Redundancy	4.22

Crystallization Conditions

crystal ID	method	pH	temperature	details
1