2C64

MAO inhibition by rasagiline analogues

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-1
Synchrotron site	ESRF
Beamline	ID14-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	C 2 2 2
Unit cell lengths	140.867, 221.114, 86.285
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 2.200
R-factor	0.223
Rwork	0.222
R-free	0.26000
Structure solution method	OTHER
RMSD bond length	0.016
RMSD bond angle	1.526
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	15.000
High resolution limit [Å]	2.200
Rmerge	0.090
Number of reflections	65730
<I/σ(I)>	9.3
Completeness [%]	99.0
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1