2BZX
Atomic model of CrkL-SH3C monomer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-08 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 53.285, 53.285, 51.193 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.3173 |
Rwork | 0.317 |
R-free | 0.37430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1uec |
RMSD bond length | 0.012 |
RMSD bond angle | 1.982 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.100 | 1.000 |
Number of reflections | 2035 | |
<I/σ(I)> | 34.3 | 3.2 |
Completeness [%] | 99.6 | 99.5 |
Redundancy | 38.8 | 26.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 1.7M AMMONIUM SULPHATE, 25.5% W/V PEG 8000, 0.085M SODIUM CACODYLATE PH6.5, 15% V/V GLYCEROL, pH 6.50 |