2BXD
Human serum albumin complexed with warfarin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2003-09-30 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 55.022, 55.358, 119.591 |
| Unit cell angles | 81.14, 90.53, 64.79 |
Refinement procedure
| Resolution | 49.320 - 3.050 |
| R-factor | 0.213 |
| Rwork | 0.213 |
| R-free | 0.25900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e78 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.300 | 3.210 |
| High resolution limit [Å] | 3.050 | 3.050 |
| Rmerge | 0.060 | 0.370 |
| Number of reflections | 23406 | |
| <I/σ(I)> | 8.9 | 2.3 |
| Completeness [%] | 97.7 | 97 |
| Redundancy | 1.9 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.00 |
