2BWH
Laue Structure of a Short Lived State of L29W Myoglobin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 288 |
| Detector technology | IMAGE PLATE |
| Collection date | 2003-12-20 |
| Detector | MARRESEARCH |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.870, 91.870, 46.040 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.000 - 1.900 |
| R-factor | 0.2299 |
| Rwork | 0.230 |
| R-free | 0.23250 |
| Structure solution method | OTHER |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.970 |
| Data reduction software | Precognition |
| Data scaling software | Epinorm |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.000 | 1.940 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 17619 | |
| Completeness [%] | 100.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.8 | pH 7.80 |
