2BWB
Crystal structure of the UBA domain of Dsk2 from S. cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-05-11 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 116.311, 44.069, 111.525 |
Unit cell angles | 90.00, 114.87, 90.00 |
Refinement procedure
Resolution | 101.020 - 2.300 |
R-factor | 0.246 |
Rwork | 0.243 |
R-free | 0.30700 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.150 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.500 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.090 | 0.280 |
Number of reflections | 23134 | |
<I/σ(I)> | 16.4 | 3.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 4 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.6 M TRISODIUM CITRATE PH 7.0 |