2BV7
Crystal structure of GLTP with bound GM3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-08 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.500, 34.600, 58.300 |
| Unit cell angles | 90.00, 116.50, 90.00 |
Refinement procedure
| Resolution | 52.200 - 1.790 |
| R-factor | 0.193 |
| Rwork | 0.189 |
| R-free | 0.25700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1tfj |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.359 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.080 | 0.520 |
| Number of reflections | 115280 | |
| <I/σ(I)> | 16.6 | 4.2 |
| Completeness [%] | 99.5 | 99.7 |
| Redundancy | 6 | 6.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
