Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ELLIOTT GX-6 |
| Temperature [K] | 292 |
| Detector technology | FILM |
| Collection date | 1981-01-01 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 317.270, 304.030, 184.600 |
| Unit cell angles | 90.00, 94.36, 90.00 |
Refinement procedure
| Resolution | 7.500 - 2.450 |
| Rwork | 0.273 |
| Structure solution method | OTHER |
| RMSD bond length | 0.016 |
| RMSD bond angle | 29.700 * |
| Data reduction software | FILME |
| Data scaling software | PURDUE (DATA PROCESSING PACKAGE) |
| Refinement software | FRODO |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.730 |
| High resolution limit [Å] | 2.450 |
| Rmerge | 0.140 |
| Number of reflections | 503000 |
| Completeness [%] | 76.0 |
| Redundancy | 1.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 6.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | virus | 10-12 (g/l) | |
| 2 | 1 | 1 | 1 (mM) | ||
| 3 | 1 | 1 | sodium phosphate | 50 (mM) |
