2BTD
Crystal structure of DhaL from E. coli
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 110 |
| Collection date | 2004-12-20 |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 139.030, 139.030, 139.030 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.400 - 2.600 |
| R-factor | 0.237 |
| Rwork | 0.235 |
| R-free | 0.27600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1un8 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.546 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.400 | 2.810 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.080 | 0.360 |
| Number of reflections | 14672 | |
| <I/σ(I)> | 27.15 | 7.7 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 16.4 | 11.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.01 M MAGNESIUM SULPHATE 0.05 M SODIUM CACODYLATE PH 6.0 1.8 M LITHIUM SULPHATE |
