2BLJ
Structure of L29W MbCO
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR591 |
| Temperature [K] | 295 |
| Detector technology | AREA DETECTOR |
| Collection date | 2003-09-12 |
| Detector | BRUKER MULTIWIRE |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.870, 91.870, 46.040 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 50.000 - 1.800 |
| R-factor | 0.2238 |
| Rwork | 0.224 |
| R-free | 0.25680 |
| Structure solution method | OTHER |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.015 |
| Data reduction software | SAINT |
| Data scaling software | SAINT |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.880 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.050 | 0.240 |
| Number of reflections | 73405 | |
| <I/σ(I)> | 11 | 3 |
| Completeness [%] | 80.0 | 61 |
| Redundancy | 4.5 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.8 | pH 7.80 |
