2BKB
q69e-FeSOD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.500, 107.700, 84.200 |
| Unit cell angles | 90.00, 95.02, 90.00 |
Refinement procedure
| Resolution | 19.970 - 1.700 |
| R-factor | 0.207 |
| Rwork | 0.207 |
| R-free | 0.23100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | WT-FESOD 1ISB.PDB |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.200 |
| Data reduction software | HKL |
| Data scaling software | HKL |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.600 |
| Rmerge | 0.070 |
| Number of reflections | 87786 |
| Completeness [%] | 86.3 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
