2ARO

Crystal Structure Of The Native Histone Octamer To 2.1 Angstrom Resolution, Crystalised In The Presence Of S-Nitrosoglutathione

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX10.1
Synchrotron site	SRS
Beamline	PX10.1
Temperature [K]	100
Detector technology	CCD
Collection date	2005-04-04
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.98
Spacegroup name	P 65
Unit cell lengths	158.084, 158.084, 101.037
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.100
R-factor	0.1859
Rwork	0.184
R-free	0.22508
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1tzy
RMSD bond length	0.020
RMSD bond angle	1.674
Data reduction software	MOSFLM
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	2.100
Number of reflections	81294

Crystallization Conditions

crystal ID	method	pH	temperature	details
1