2AR3
E90A mutant structure of PlyL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-12-16 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 61 |
Unit cell lengths | 163.644, 163.644, 38.462 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.830 - 2.200 |
R-factor | 0.226 |
Rwork | 0.226 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 27787 |
Completeness [%] | 91.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 298 | 0.6 M NaH2PO4, 1.0 M K2HPO4, 0.1 M acetate at pH 6.7, VAPOR DIFFUSION, SITTING DROP, temperature 298K |