2ANA
THE CRYSTAL STRUCTURE OF D(G-G-G-G-C-C-C-C). A MODEL FOR POLY(DG).POLY(DC)
Experimental procedure
| Temperature [K] | 291 |
| Detector technology | DIFFRACTOMETER |
| Detector | ENRAF-NONIUS CAD4 |
| Spacegroup name | P 61 |
| Unit cell lengths | 45.320, 45.320, 42.250 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.500 |
| R-factor | 0.14 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 0.024 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 2215 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | slow evaporation * | 6.8 * | 7 * | VAPOR DIFFUSION, temperature 280.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | NA CACODYLATE | ||
| 3 | 1 | 1 | MGCL2 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | octamer duplex | 0.8 (mM) | ||
| 2 | 1 | sodium cacodylate | 30 (mM) |
