2AEU
MJ0158, apo form
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-04-05 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9796, 0.9808, 0.95 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 58.065, 72.991, 82.782 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.000 - 1.700 |
R-factor | 0.21088 |
Rwork | 0.208 |
R-free | 0.25944 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.769 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.000 | 1.800 |
High resolution limit [Å] | 1.650 | 1.700 |
Number of reflections | 37208 | |
Completeness [%] | 92.0 | 85.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 2.2 | 293 | PEG400, ammonium sulfate, pH 2.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 2.2 | 293 | PEG400, ammonium sulfate, pH 2.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 2.2 | 293 | PEG400, ammonium sulfate, pH 2.2, VAPOR DIFFUSION, SITTING DROP, temperature 293K |