2A7F

On the Routine Use of Soft X-Rays in Macromolecular Crystallography, Part III- The Optimal Data Collection Wavelength

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 5.2R
Synchrotron site	ELETTRA
Beamline	5.2R
Temperature [K]	100
Spacegroup name	P 43 21 2
Unit cell lengths	78.710, 78.710, 37.210
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 1.850
R-factor	0.168
Rwork	0.166
R-free	0.23200
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.021
RMSD bond angle	1.745
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	1.850
Number of reflections	10173

Crystallization Conditions

crystal ID	method	pH	temperature	details
1