292D
INTERACTION BETWEEN THE LEFT-HANDED Z-DNA AND POLYAMINE:THE CRYSTAL STRUCTURE OF THE D(CG)3 AND N-(2-AMINOETHYL)-1,4-DIAMINOBUTANE COMPLEX
Experimental procedure
| Detector technology | DIFFRACTOMETER |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 17.940, 31.230, 44.550 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.000 |
| R-factor | 0.161 |
| Starting model (for MR) | ZDF001 |
| RMSD bond length | 0.014 * |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | pH 7.00, VAPOR DIFFUSION |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MGCL2 | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | N-(2-AMINOETHYL)-1,4-DIAMINOBUTANE_HCL |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | ammonium salt | 2 (mM) | |
| 2 | 1 | drop | PA(24) trichloride | 10 (mM) | |
| 3 | 1 | drop | 15 (mM) | ||
| 4 | 1 | drop | sodium ccacodylate | 30 (mM) |
