270D
STRUCTURAL STUDIES ON NUCLEIC ACIDS
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1995-05-17 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.828, 40.323, 65.563 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.010 |
R-factor | 0.176 |
Structure solution method | MIR |
RMSD bond length | 0.024 |
RMSD bond angle | 0.050 |
Data reduction software | RIGAKU |
Data scaling software | RIGAKU |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.200 |
High resolution limit [Å] | 2.010 |
Rmerge | 0.082 |
Number of reflections | 8707 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.1 | pH 7.10 |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA CACODYLATE |