26AY
Crystal structure of SchOMT2-SAM-GOM from Schisandra chinensis
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2025-06-28 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 43 2 2 |
| Unit cell lengths | 95.740, 95.740, 181.650 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 18.780 - 2.430 |
| R-factor | 0.2149 |
| Rwork | 0.212 |
| R-free | 0.26360 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.993 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 95.870 | 2.330 |
| High resolution limit [Å] | 2.210 | 2.210 |
| Rpim | 0.078 | |
| Number of reflections | 42246 | 6211 |
| <I/σ(I)> | 7.4 | 0.8 |
| Completeness [%] | 97.2 | 100 |
| Redundancy | 19.6 | 14.8 |
| CC(1/2) | 0.995 | 0.448 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.2M (Ca(CH3COO)2.H2O 0.1M Sodium cacodylate pH6.5 38%PEG400 |
