239D
POLYMORPHISM IN LEFT HANDED DNA: THE CRYSTAL STRUCTURE OF D(CCCGGG)2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Detector technology | DIFFRACTOMETER |
| Detector | ENRAF-NONIUS CAD4 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 17.764, 30.925, 43.922 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.050 |
| R-factor | 0.212 |
| Rwork | 0.212 |
| R-free | 0.35200 |
| RMSD bond length | 0.030 |
| RMSD bond angle | 5.700 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Number of reflections | 1704 |
| Completeness [%] | 44.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.98 | 296 | pH 6.98, VAPOR DIFFUSION, HANGING DROP, temperature 296.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | BACL2 | ||
| 3 | 1 | 1 | SPERMINE | ||
| 4 | 1 | 1 | NA CACODYLATE | ||
| 5 | 1 | 2 | WATER | ||
| 6 | 1 | 2 | MPD |
