1W1I
Crystal structure of dipeptidyl peptidase IV (DPPIV or CD26) in complex with adenosine deaminase
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-09-30 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 158.065, 168.504, 236.842 |
格子定数 [度] | 90.00, 100.54, 90.00 |
精密化法
残基 | 30.000 - 3.030 |
R因子 | 0.224 |
Rwork | 0.224 |
R-free | 0.25700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1N1M AND 1KRM |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.340 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.9999) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 3.150 |
分解能 [Å] (高) | 3.030 | 3.030 |
Rmerge_l_obs | 0.090 | 0.400 |
独立反射数 | 100817 | |
<I/σ(I)> | 10 | 2.1 |
完全性 [%] | 85.3 | 81.3 |
冗長性 | 2.3 | 2.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 8 | pH 8.00 |