Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1VPS

POLYOMAVIRUS VP1 PENTAMER COMPLEXED WITH A DISIALYLATED HEXASACCHARIDE

Experimental procedure
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]120
Detector technologyIMAGE PLATE
Collection date1996-02
DetectorFUJI
Spacegroup nameP 31 2 1
格子定数 [Å]221.500, 221.500, 99.800
格子定数 [度]90.00, 90.00, 120.00
精密化法
残基20.000 - 1.900
R因子0.177
Rwork0.177
R-free0.20500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)UNCOMPLEXED VP1 PENTAMER (PDB ENTRY 1VPN)
結合長の平均二乗偏差(RMSD) [Å]0.007
結合角の平均二乗偏差(RMSD) [度]1.350
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)25.0002.000
分解能 [Å] (高)1.9001.900
Rmerge_l_obs0.058

*

独立反射数188556
<I/σ(I)>14.52.1
完全性 [%]85.656.5
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

*

8DROP: 1.0 M AMMONIUM PHOSPHATE PH 8.0 2.5 & ETHANOL 8-10 MG/ML PROTEIN RESERVOIR: 2.0 M AMMONIUM PHOSPHATE PH 8.0 5 % ETHANOL
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropammonium phosphate1.0 (M)
21dropethanol2.5 (%)
31dropprotein8-10 (mg/ml)
41reservoirammonium phosphate2.0 (M)
51reservoirethanol5 (%)

225158

件を2024-09-18に公開中

PDB statisticsPDBj update infoContact PDBjnumon