1UYE
Human Hsp90-alpha with 8-(2-chloro-3,4,5-trimethoxy-benzyl)-9-pent-4-ylnyl-9H-purin-6-ylamine
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-01-15 |
Detector | RAXIS IV |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 66.700, 90.755, 98.171 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 67.420 - 2.000 |
Rwork | 0.183 |
R-free | 0.21814 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yer |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 2.100 |
分解能 [Å] (高) | 2.000 | 2.000 |
Rmerge_l_obs | 0.092 | 0.352 |
独立反射数 | 46520 | |
<I/σ(I)> | 6.8 | 1 |
完全性 [%] | 93.6 | 72.1 |
冗長性 | 2.4 | 2.1 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 6.5 | 25% PEG MME 2000, 0.1M NA CACODYLATE, PH6.5, 0.2M MGCL2., pH 6.50 |