1URJ
Single stranded DNA-binding protein(ICP8) from Herpes simplex virus-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-03-15 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 100.910, 145.370, 162.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.000 |
R-factor | 0.235 |
Rwork | 0.235 |
R-free | 0.28570 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.360 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 20.000 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.090 | 0.300 |
Number of reflections | 47265 | |
<I/σ(I)> | 9.8 | 2.98 |
Completeness [%] | 98.0 | 97 |
Redundancy | 3.9 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 12% PEG 3K, 0.1 M SODIUM/POTASSIUM PHASPHATE PH 6.0 |