1SFT
ALANINE RACEMASE
Experimental procedure
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 1994-11-26 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 98.590, 90.130, 85.130 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 10.000 - 1.900 |
R因子 | 0.193 |
Rwork | 0.193 |
R-free | 0.26700 |
結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
結合角の平均二乗偏差(RMSD) [度] | 26.050 * |
Data reduction software | RIGAKU |
Data scaling software | RIGAKU |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 10.000 |
分解能 [Å] (高) | 1.900 |
Rmerge_l_obs | 0.046 |
独立反射数 | 52379 |
<I/σ(I)> | 9.3 |
完全性 [%] | 83.0 |
冗長性 | 3.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, sitting drop * | 8.5 | pH 8.5 |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | protein | 30 (mg/ml) | |
2 | 1 | drop | PEG4000 | 30 (%(w/v)) | |
3 | 1 | drop | sodium acetate | 200 (mM) | |
4 | 1 | drop | Tris-HCl | 100 (mM) | |
5 | 1 | reservoir | PEG4000 | 30 (%(w/v)) | |
6 | 1 | reservoir | sodium acetate | 200 (mM) | |
7 | 1 | reservoir | Tris-HCl | 100 (mM) |