1S32
Molecular Recognition of the Nucleosomal 'Supergroove'
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-05-25 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.1 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 105.352, 109.717, 181.827 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 100.000 - 2.050 |
Rwork | 0.219 |
R-free | 0.24340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aoi |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.099 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS (1.0) |
Refinement software | CNS (1.0) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 100.000 | 2.100 |
分解能 [Å] (高) | 2.050 | 2.050 |
Rmerge_l_obs | 0.076 | 0.353 |
独立反射数 | 124523 | |
<I/σ(I)> | 22.99 | 2.04 |
完全性 [%] | 94.4 | 54.1 |
冗長性 | 4.75 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 292 | Manganese chloride, potassium chloride, potassium cacodylate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 292K |
結晶化試薬
ID | 結晶ID | 濃度 | 試薬名 | 濃度 (単位) | 詳細 |
1 | 1 | 1 | Manganese chloride | ||
2 | 1 | 1 | potassium chloride | ||
3 | 1 | 1 | potassium cacodylate | ||
4 | 1 | 1 | H2O | ||
5 | 1 | 2 | Manganese chloride | ||
6 | 1 | 2 | potassium chloride | ||
7 | 1 | 2 | H2O |