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1RS8

Bovine endothelial NOS heme domain with D-lysine-D-nitroarginine amide bound

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL7-1
Synchrotron siteSSRL
BeamlineBL7-1
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-04-04
DetectorMARRESEARCH
Wavelength(s)1.08
Spacegroup nameP 21 21 21
Unit cell lengths57.009, 106.215, 156.536
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution46.830 - 2.300
R-factor0.222
Rwork0.222
R-free0.27600
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.008
RMSD bond angle1.500
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.340
High resolution limit [Å]2.3002.300
Rmerge0.0720.646
Number of reflections42229
<I/σ(I)>19.52
Completeness [%]97.098.9
Redundancy4.54
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.5280PEG 3350, MgOAc, Na Cacodylate, TCEP, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 280K

225158

数据于2024-09-18公开中

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