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1RKC

Human vinculin head (1-258) in complex with talin's vinculin binding site 3 (residues 1944-1969)

Experimental procedure
実験手法MIRAS
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Detector technologyCCD
Wavelength(s)0.9793,1.2545,0.9793
Spacegroup nameI 41 3 2
格子定数 [Å]155.680, 155.680, 155.680
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基15.000 - 2.700
Rwork0.244
R-free0.33500
Structure solution methodSAD
結合長の平均二乗偏差(RMSD) [Å]0.010
結合角の平均二乗偏差(RMSD) [度]1.263
Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwareSHARP
Refinement softwareBUSTER-TNT
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)45.000

*

分解能 [Å] (高)2.7002.800

*

Rmerge_l_obs0.100

*

0.497

*

Total number of observations178681

*

独立反射数90511290

*

完全性 [%]99.8

*

99.7

*

冗長性19.6

*

5.4

*

結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion

*

42932% MPD; 100 mM citric acid (pH 4); 100 mM CdCl2, pH 4.0, temperature 293K
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11reservoirMPD2 (%)
21reservoircitric acid100 (mM)pH4
31reservoir100 (mM)

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件を2024-09-18に公開中

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