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1QS1

CRYSTAL STRUCTURE OF VEGETATIVE INSECTICIDAL PROTEIN2 (VIP2)

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]103
Detector technologyCCD
Collection date1997-12-30
DetectorMARRESEARCH
Spacegroup nameP 1
格子定数 [Å]53.900, 78.700, 105.900
格子定数 [度]108.65, 89.96, 90.02
精密化法
残基20.000 - 1.500
R因子0.235
Rwork0.235
R-free0.26900
結合長の平均二乗偏差(RMSD) [Å]0.006
結合角の平均二乗偏差(RMSD) [度]1.300
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMLPHARE
Refinement softwareCNS
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)20.0001.550
分解能 [Å] (高)1.5001.500
Rmerge_l_obs0.0460.270
Total number of observations468627

*

独立反射数215237
<I/σ(I)>13
完全性 [%]83.469.2
冗長性2.21.6
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion

*

7.520

*

PEG200, BOG, IMIDAZOLE, MALATE, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropprotein20 (mg/ml)
21dropTris20 (mM)
31reservoirPEG20030 (%(w/v))
41reservoiroctyl-beta-D-glucopyranoside1 (%(w/v))
51reservoirimidazole/malate200 (mM)

225158

件を2024-09-18に公開中

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