1LNF
A structural analysis of metal substitutions in thermolysin
Experimental procedure
実験手法 | SINGLE CRYSTAL |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | MULTIWIRE AREA DETECTOR |
Detector | XUONG-HAMLIN |
Spacegroup name | P 61 2 2 |
格子定数 [Å] | 93.850, 93.850, 131.400 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 20.000 - 1.700 |
R因子 | 0.152 |
Structure solution method | MOLECULAR SUBSTITUTION |
結合長の平均二乗偏差(RMSD) [Å] | 0.015 |
結合角の平均二乗偏差(RMSD) [度] | 2.000 |
Data reduction software | XENGEN ((HOWARD) |
Data scaling software | XENGEN ((HOWARD) |
Refinement software | TNT |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | unknown * | 7.2 | Holmes, M.A., (1982) J.Mol.Biol., 160, 623. * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | 1 | 2.5 (M) | ||
2 | 1 | 2 | calcium acetate | 0.01 (M) | |
3 | 1 | 2 | Tris | 0.01 (M) | |
4 | 1 | 2 | dimethyl sulphoxide | 7 (%(v/v)) |