1LDC
X-RAY STRUCTURE OF TWO COMPLEXES OF THE Y143F FLAVOCYTOCHROME B2 MUTANT CRYSTALLIZED IN THE PRESENCE OF LACTATE OR PHENYL-LACTATE
Experimental procedure
Collection date | 1993-01-08 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 164.500, 164.500, 114.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 6.000 - 2.900 |
R-factor | 0.195 |
Rwork | 0.195 |
RMSD bond length | 0.010 |
RMSD bond angle | 3.700 |
Data reduction software | MOSFLM |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 * |
High resolution limit [Å] | 2.900 * |
Rmerge | 0.150 |
Total number of observations | 156473 * |
Number of reflections | 30412 |
Completeness [%] | 80.0 |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.5 * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 10-12 (%(w/w)) | |
2 | 1 | reservoir | MES | 50 (mM) |