1LDC
X-RAY STRUCTURE OF TWO COMPLEXES OF THE Y143F FLAVOCYTOCHROME B2 MUTANT CRYSTALLIZED IN THE PRESENCE OF LACTATE OR PHENYL-LACTATE
Experimental procedure
Collection date | 1993-01-08 |
Spacegroup name | P 32 2 1 |
格子定数 [Å] | 164.500, 164.500, 114.000 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 6.000 - 2.900 |
R因子 | 0.195 |
Rwork | 0.195 |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 3.700 |
Data reduction software | MOSFLM |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Quality characteristics
Overall | |
分解能 [Å] (低) | 100.000 * |
分解能 [Å] (高) | 2.900 * |
Rmerge_l_obs | 0.150 |
Total number of observations | 156473 * |
独立反射数 | 30412 |
完全性 [%] | 80.0 |
冗長性 | 7.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion * | 5.5 * | 20 * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | reservoir | PEG4000 | 10-12 (%(w/w)) | |
2 | 1 | reservoir | MES | 50 (mM) |