1KU0
Structure of the Bacillus stearothermophilus L1 lipase
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| 格子定数 [Å] | 119.620, 85.040, 98.360 |
| 格子定数 [度] | 90.00, 99.73, 90.00 |
精密化法
| 残基 | 99.000 - 2.000 |
| Rwork | 0.185 |
| R-free | 0.21800 |
| Structure solution method | MIR |
| Phasing software | SHARP |
| Refinement software | CNS (0.9) |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (高) | 2.000 | 2.000 |
| Rmerge_l_obs | 0.059 | 0.222 |
| <I/σ(I)> | 20.2 | 6.1 |
| 完全性 [%] | 96.9 | 95.2 |
| 冗長性 | 3 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 |
