1KRQ
CRYSTAL STRUCTURE ANALYSIS OF CAMPYLOBACTER JEJUNI FERRITIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Temperature [K] | 296 |
Detector technology | IMAGE PLATE |
Collection date | 2000-04-17 |
Detector | MARRESEARCH |
Wavelength(s) | 0.966 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 152.050, 152.050, 152.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.700 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fha |
RMSD bond length | 0.006 |
RMSD bond angle | 1.050 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 2.770 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 8373 | |
<I/σ(I)> | 5.9 | 2 |
Completeness [%] | 98.5 | 99.8 |
Redundancy | 6.5 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 300 | Ammonium sulfate, PEG400, Hepes, Sodium azide, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 300K |