1JSU
P27(KIP1)/CYCLIN A/CDK2 COMPLEX
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1996-02-20 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.800, 78.300, 137.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.300 |
R-factor | 0.192 * |
Rwork | 0.192 |
R-free | 0.26000 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.450 |
Data reduction software | HKL |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.056 |
Total number of observations | 162339 * |
Number of reflections | 34683 * |
Completeness [%] | 96.1 |
Redundancy | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 * | 4 * | drop solution was mixed with an equal volume of reservoir solution * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 30 (mg/ml) | |
2 | 1 | drop | HEPES | 40 (mM) | |
3 | 1 | drop | 200 (mM) | ||
4 | 1 | drop | dithiothreitol | 5 (mM) | |
5 | 1 | reservoir | ammonium sulfate | 35 (%sat) | |
6 | 1 | reservoir | HEPES | 40 (mM) | |
7 | 1 | reservoir | dithiothreitol | 5 (mM) |