1GZ8
HUMAN CYCLIN DEPENDENT KINASE 2 COMPLEXED WITH THE INHIBITOR 2-Amino-6-(3'-methyl-2'-oxo)butoxypurine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1998-04-25 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.860, 71.070, 71.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.640 - 1.300 |
R-factor | 0.153 |
Rwork | 0.151 |
R-free | 0.18500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e1v |
RMSD bond length | 0.020 |
RMSD bond angle | 1.910 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.360 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.046 | 0.471 |
Number of reflections | 63538 | |
<I/σ(I)> | 20.2 | 1.8 |
Completeness [%] | 96.3 | 97.2 |
Redundancy | 2.3 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 7.4 | Lawrie, A.M., (1997) Nat.Struct.Biol., 4, 796. * |