1G6K

Crystal structure of glucose dehydrogenase mutant E96A complexed with NAD+

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2 Å)

Cell axes121.95566.640120.065
Cell angles90.0093.4490.00
SpacegroupC 1 2 1
Resolution limits39.95 - 2.00
the highest resolution shell value -
R-work0.21900
R-free0.23800
RMSD bond length0.006
RMSD bond angle1.180

Data Collection Statistics

Resolution limits100.00 - 2.00
the highest resolution shell value -
Number of reflections294512
Rmerge_l_obs0.076
the highest resolution shell value0.208
Completeness94.6
Redundancy4.78
the highest resolution shell value2.2
I/sigma(I)2

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP6293

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*