1CJP
CONCANAVALIN A COMPLEX WITH 4'-METHYLUMBELLIFERYL-ALPHA-D-GLUCOPYRANOSIDE
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-11-30 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 81.620, 128.710, 82.230 |
Unit cell angles | 90.00, 118.47, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.780 |
R-factor | 0.182 |
Rwork | 0.182 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vam |
RMSD bond length | 0.008 |
RMSD bond angle | 1.900 |
Data reduction software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 * | |
High resolution limit [Å] | 2.780 * | 2.780 * |
Rmerge | 0.074 | 0.238 * |
Total number of observations | 151116 * | |
Number of reflections | 37358 | |
Completeness [%] | 99.0 | 95.2 * |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 70 (mg/ml) | |
2 | 1 | reservoir | Tris | 10 (mM) | |
3 | 1 | reservoir | ammonium sulfate | 1 (M) |